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marine science

SEM-EDS Laboratory

The SEM-EDS Laboratory houses a TESCAN VEGA 3 LMU high-performance, Variable Pressure Analytical SEM with LAB6 having high resolution of 2 nm, along with the most advanced LN2-free high-resolution, high-speed EDS (QUANTAX 200 with XFlash®6/30 SDD Detector) from Bruker with Energy resolution < 126 eV and a 30 mm2 active window area. It is also equipped with SE, R-BSE, Colour + Panchromatic Cathodoluminescence (CL) Detectors with digital image processing and storage capabilities.

 

The SEM-EDS is capable of capturing ultra structural details of samples as images in digital mode which in turn permits the observation and characterization of heterogeneous organic and inorganic materials, thereby providing high-resolution and high depth-of-field images of sample surface and near-surface. The instrument can magnify specimens up to 10,00,000 times. SE Detector provides Topographic Contrast Imaging using Secondary Electrons. Retractable BSE detectors with YAG scintillator provides compositional contrast, material contrast, phase contrast imaging and phase Identification using Back Scattered Electrons.

 

The state of the art EDS facility provides qualitative and semi quantitative compositional analysis of different phases, grains and selected points of the samples including Multi Point, Line Scan and elemental mapping of the selected area. Elements from Be (5) to Americium (95) with a detection limit of 1000 ppm can be analyzed. Conductive coatings of gold or carbon is deposited for sample preparation of non-conducting samples using a Quorum SC7620 sputter coater or Quorum CA7625 evaporative carbon coater.

Samples of rocks, minerals, fossils, ores, biological, pharmaceutical, metallurgical, polymer materials can be studied using SEM-EDS facility. NCESS primarily uses the equipment for mineralogical investigations, petrological studies, characterisation of palaeontological samples and interpretation of sedimentological and depositional environments.

Contact:

Dr. Tomson J Kallukalam

Scientist-In-Charge

T: 0471-2511669

E: This email address is being protected from spambots. You need JavaScript enabled to view it.

Download SEM-EDS Requisition form

marine science

X-ray diffraction (XRD)

X-ray diffraction (XRD) is a rapid analytical technique primarily used for phase identification of a crystalline material and can provide information on unit cell dimensions. X-ray diffraction is most widely used for the identification of unknown crystalline materials (e.g. minerals, inorganic compounds). Determination of unknown solids is critical to various geological applications.

xrd-lab-thumbXRD measures the intensities of a reflected X-Ray beam from a small area. Atomic-level spacing within the crystal lattice of the specimen can be obtained by the results. This helps us in understanding details of the crystal structure for the substance. XRD helps in identifying different phases with identical compositions with finer details of the crystal structure, such as the state of atomic “order”. In addition, strain analysis and determination of the degree of crystallization can also be assessed. Due to this versatility XRD finds wide range of applications in geology, material science, environmental science, chemistry, forensic science, pharmaceutical industry and others.

 

The XRD facility at NCESS, commissioned in 2006, consists of a PANalytical 3 kW X’pert PRO X-ray diffractometer. NCESS primarily uses the facility in geological application, few which are in Environmental Studies, mineral identification and genesis, stratigraphic analysis and in mineral-resource assessments. Few Other applications include:

  • Characterization of crystalline materials
  • Identification of fine-grained minerals such as clays and mixed layer clays that are difficult to determine optically
  • Determination of unit cell dimensions
  • Measurement of sample purity.

Contact:

Group Head, MGG

Scientist-In-Charge

T: 0471-2511668/1669/1504

E: This email address is being protected from spambots. You need JavaScript enabled to view it.

Download XRD Analysis Request form

marine science

Sedimentology Laboratory (SL)

sedimentology-laboratory-219x150The sedimentology laboratory is one of the core laboratories of NCESS since its inception. The laboratory has facility for both wet and dry sample analysis. The wet analysis includes the preparation of samples for textural, mineralogical, geochemical and clay mineralogical analysis. The laboratory has a deep freezer for storing and archiving the sediment samples and sediment cores. The laboratory is used extensively by the research students/project fellows and at a given time more than 5-6 persons work in the laboratory. The laboratory is opened even during the late hours for the students to complete the work. The dry unit of the laboratory has a facility for sieving the sediment samples for grain size distribution.

marine science

Field Research Facility (FRF)

The Field Research Facility established at Valiathura, near Thiruvananthapuram is equipped with facilities for collection of coastal environmental data for various projects. The important facilities available are Valeport wave gauge, anemograph and automatic video camera. The pier jetting out into the sea for a length of roughly 100-m from the shoreline is a very useful platform for installation of equipments and for making littoral environmental observations. A wave rider buoy has also been installed in the shallow waters off Trivandrum under a project funded by the INCOIS, Hyderabad. The Datawell Directional Waverider buoy measures the wave height and period by measuring the vertical acceleration by means of an accelerometer placed on a gravity stabilized platform and by double integrating the acceleration to get the displacement. The direction of wave approach is measured based on the translational principle.The data from the buoy are transmitted through VHF/GSM/INSAT-1C satellite system to the shore station located at CESS Thiruvananthapuram at synoptic hours. The data transmission is at every three hour interval. Also, the data from GPS mounted on the wave rider buoy can be used to monitor the position of the buoy continuously and in tracking the buoy. The data received from the buoy would be then sent on real-time to INCOIS, Hyderabad for further dissemination to the operational users such as India Meterological Dept (IMD), Coast Guard (CG), INCOIS, Navy, ONGC and other agencies.

FRF

The data will be disseminated to the fishermen and coastal community by organising workshops and by employing methods of mass communication like television, radio, news paper, VHF, etc. The real time validation of sea state forecast for the Kerala coast will be carried out by INCOIS. Further, the dissemination of sea state conditions and potential fishing zone through electronic display board being established at Vizhinjam fishing harbour and other important fishing harbours.

marine science

Field Instrumentation (FI)

The Division has state-of-the art oceanographic and survey equipments required for acquisition of field data for implementation of different projects of the Division. Some of these are:

Acoustic Doppler Current Profiler (ADCP)

ADCP-215x150An Acoustic Doppler Current Profiler (ADCP) measures current speed and direction by transmitting high-frequency bursts of sound though the water column. Particles in the water column scatter the sound back to the ADCP, which listens for these echoes, records them as data, and labels the different depths from which they have returned. Motion of the particles in the water column (such as movement with the current) causes the echoes to change in frequency. The ADCP measures this change, the Doppler shift, to determine current speed and direction at the different depths in the water column. The ADCP can measure current velocities through the water column either looking vertically downwards or vertically upwards. The measurement can be from a moving boat for synoptic current measurement of a large area or moored on the seabed.

Valeport & Dobie Wave Gauge

valeportdobie-wave-gauge-182x150Valeport is also called as Directional Wave Recorder used for measuring waves and tides with a direction measuring mechanism called a flux gate compass and Valeport 2-axis EM current sensor. It has a range of 0 to 360° with accuracy ±1° and resolution 0.1°. It performs full onboard directional data analysis, allowing real time directional information at an unsurpassed 2° resolution. It is a cost-effective solution to directional wave monitoring requirements in all shallow water coastal applications. The current sensor works in the range ±5 m/s with accuracy of ±1% and a resolution 0.001m/s. This “PUV” type wave recorder use Linear Wave Theory to analyse the pressure and current oscillations generated by the wave action. The data processing is all carried out on board, giving you descriptive statistics, energy spectra, and high resolution directional spectra all in real time. All the raw data is logged as well, so it can be used in customised post-processing routines as well.

Dobie Wave Gauge is a self-recording system based on a pressure sensor to measure waves and water level changes. The Dobie is mounted inside a cylindrical steel housing welded to a steel gate that provided a stable platform resistant to sinking into the sea floor. When waves are passing overhead the Dobie deployed at the seabed, the fluctuating pressure, associated with the rising and falling of water, is recorded by the instrument. The fluctuations in pressure due to waves actually decrease in amplitude with depth below the mean water level (MWL), and the rate of decrease with depth depends on the wave period. Thus, pressure under long period waves can be readily felt, and measured at depth, but pressure fluctuations under short-period waves may not actually penetrate to the same depth.

S4 Current Meter:

S4currentMeter-182x150S4 Current meter (spherical yellow colour) attached to stainless steel frame. The Dobie wave gauge is also seen attached to the same frame at one corner.

S4-Current meter – an electromagnetic current meter manufactured by InterOcean – is used to record near-bed water velocities. The S4 is designed to measure true magnitude and direction of horizontal current motion in any water environment. Water flows through the electromagnetic field created by the instrument, produces a voltage (potential gradient), which is proportional to the magnitude of the water velocity past the sensor. This voltage is then sensed by the two pairs of titanium electrodes located symmetrically on the equator of the sensor.

Shallow Seismic Profiler

shallow-seismic-profiler-182x150The Shallow Seismic Profiler or FM Sub Bottom Profiler manufactured by M/s. Edge Tech, USA is a versatile field instrument used for studying the stratigraphic structure and nature of the bottom sediments in the water bodies. It generates cross-sectional images of the seabed or lake and collects digital normal incidence reflection data over frequency range 2 to 16 kHz.

The sub-bottom profiler system consists of three components viz., the deck unit consisting of processor, amplifier, monitor, keyboard and track ball and the under water unit consisting of underwater cable and a towed vehicle. A 12-bit D/A converter generate the FM pulse. This FM signal is amplified approximately to100 V p-p by linear power amplifier in the deck unit. A piston transducer source converts the high voltage signal to an acoustic pulse. The acoustic returns from the sea floor are measured with the receiving array. The preamplifier mounted on the tow vehicle amplifies the output of the receiving array. A digital matched filter compresses the FM data into a sequence of high-resolution reflections. This passes into filters to display different bands of the processed spectrum. This instrument allows the user to select two overlapping frequency bands within the total bandwidth of the tow vehicle. The sonar display shows two sub-bottom images, one for each of the selected bands. The overlapping frequency bands enable the user to observe sediment structure of the bottom in different frequency bands. The system has the ability to strip away the water bodies and provide high-resolution sub-bottom images.

Piston Corer:

piston-corer-150x150The Piston corer is a long, heavy tube with a gravity weight attached on top, that is used to collect the sediment core from sea or lakes. The corer can be operated from the mechanised boat with a davit and winch facility. Corer can operated easily in areas of soft sea or lake bottoms where the penetration is higher resulting in the recovery of long cores. The sediment cores are useful in studying the Quarternary paleoclimate, sedimentology and volcanic history.

Echo sounder:

echo-sounder-130x150Echo sounder is used for depth measurement, and preparing the bathymetric map and data input for numerical modeling. The echo sounder used in the study is a portable shallow water echo sounder capable of measuring up to a depth of 60m. It operates with a combined 35/200 kHz transducer as transmitting and receiving transducer. The transducer can be mounted at the boat’s bottom or as portable version attached on the side of the boat/vessel. It can be operated at four depth ranges :0-18m, 15-33m, 30-48m and 45-63m with an accuracy of 0.25% of selected scale range. The echo sounder uses analogue recording paper for recording the bottom echo. The analogue data can be read for the precise depths at different positions.

Differential Global Positioning System:

global-positioning-system-225x103GPS is a navigational aid, which is used to locate the position and altitude based on satellite positioning. The equipment used for position fixing initially was the Magellan GPS NAV 5000, which is manufactured by Magellan Systems Corporation, California. The NAV 5000 is generally capable of better than 100 meters horizontal accuracy in autonomous operation. It uses five channels working simultaneously to locate and collect data from the GPS satellites. The data received from the satellites is rapidly processed to compute current position, altitude, velocity and navigational data in less than one minute. Though it can compute the altitude it is not a reliable estimate. A Real Time Kinematic GPS- SR9400 with accuracy of the order of 1m was procured subsequently under the project. This is manufactured by Leica, Switzerland. It consists of two sets of receiver and controller, one as a base unit and the other as a rover unit. The real time surveying is made possible by using a radio modem, which links between the base and the rover.

Sediment Traps:

sediment-traps-197x150The sediment trap is a field instrument when deployed in the sea, provides the quantum of suspended sediment load in the seawater over a period of time. It is made of PVC pipe with a diameter of 9 cm and length 35 cm. The bottom end is closed using an end cap. Two types of sediment traps could be used. Those placed in the bottom layers or in zones of high sedimentation have a nozzle or a reducer in the top to provide a reduced opening of 4 cm. This is to take care of the anticipated higher sediment load in the bottom layers that might result in overfilling. Further from the seabed where the suspended load is less, there is no need for a nozzle. The trap, which is kept very close to the bottom, is made in such a way that it can be kept in a horizontal position with an opening on its side using a connector. The sediment traps mounted on the sensor housing are open when deployed in the sea. Before retrieval the traps are closed by sending a diver to the depth of deployment.